Solid phase extraction of uranium on a new brush type graft copolymer and spectrophotometric determination of its in water samples

A new versatile solid phase extraction and spectrophotometric determination of uranium (VI) was proposed with using poly(caprolactone-b-vinyl benzyl chloride-g-dimethyl amino ethyl methacrylate), poly(CL-b-VB-g-DMAEMA), amphiphilic brush type block/graft copolymer. The method is based on the adsorption of uranium(VI)-pyrocatechol violet complex on surface on the adsorbent. The parameters such as pH, amount of ligand and copolymer, sample volume were optimized. Detection limit, preconcentration factor and relative standard deviation were found as 0.45 µg L-1, 100 and 3.8 %, respectively. Adsorption capacity of the polymer for uranium(VI) was found 52 mg g-1. The method was applied to different water samples and standard reference materials. © 2016, Akadémiai Kiadó, Budapest, Hungary.

Dergi Adı Journal of Radioanalytical and Nuclear Chemistry
Dergi Cilt Bilgisi 310
Dergi Sayısı 3
Sayfalar 1255 - 1263
Yayın Yılı 2016
Eser Adı
[dc.title]
Solid phase extraction of uranium on a new brush type graft copolymer and spectrophotometric determination of its in water samples
Yazar
[dc.contributor.author]
Tüzen, Mustafa
Yazar
[dc.contributor.author]
Esra, Bağda
Yazar
[dc.contributor.author]
Hazer, Baki
Yayın Yılı
[dc.date.issued]
2016
Yayıncı
[dc.publisher]
Springer Netherlands
Yayın Türü
[dc.type]
article
Özet
[dc.description.abstract]
A new versatile solid phase extraction and spectrophotometric determination of uranium (VI) was proposed with using poly(caprolactone-b-vinyl benzyl chloride-g-dimethyl amino ethyl methacrylate), poly(CL-b-VB-g-DMAEMA), amphiphilic brush type block/graft copolymer. The method is based on the adsorption of uranium(VI)-pyrocatechol violet complex on surface on the adsorbent. The parameters such as pH, amount of ligand and copolymer, sample volume were optimized. Detection limit, preconcentration factor and relative standard deviation were found as 0.45 µg L-1, 100 and 3.8 %, respectively. Adsorption capacity of the polymer for uranium(VI) was found 52 mg g-1. The method was applied to different water samples and standard reference materials. © 2016, Akadémiai Kiadó, Budapest, Hungary.
Kayıt Giriş Tarihi
[dc.date.accessioned]
2019-12-23
Açık Erişim Tarihi
[dc.date.available]
2019-12-23
Yayın Dili
[dc.language.iso]
eng
Konu Başlıkları
[dc.subject]
Pyrocatechol violet
Konu Başlıkları
[dc.subject]
Solid phase extraction
Konu Başlıkları
[dc.subject]
Spectrophotometer
Konu Başlıkları
[dc.subject]
Uranium
Konu Başlıkları
[dc.subject]
Water samples
Künye
[dc.identifier.citation]
Tuzen, M., Bagda, E. ve Hazer, B. (2016). Solid phase extraction of uranium on a new brush type graft copolymer and spectrophotometric determination of its in water samples. Journal of Radioanalytical and Nuclear Chemistry, 310(3), 1255-1263. doi:10.1007/s10967-016-4949-4
Haklar
[dc.rights]
info:eu-repo/semantics/closedAccess
ISSN
[dc.identifier.issn]
0236-5731
İlk Sayfa Sayısı
[dc.identifier.startpage]
1255
Son Sayfa Sayısı
[dc.identifier.endpage]
1263
Dergi Adı
[dc.relation.journal]
Journal of Radioanalytical and Nuclear Chemistry
Dergi Sayısı
[dc.identifier.issue]
3
Dergi Cilt Bilgisi
[dc.identifier.volume]
310
Tek Biçim Adres
[dc.identifier.uri]
https://dx.doi.org/10.1007/s10967-016-4949-4
Tek Biçim Adres
[dc.identifier.uri]
https://hdl.handle.net/20.500.12628/7566
Görüntülenme Sayısı ( Şehir )
Görüntülenme Sayısı ( Ülke )
Görüntülenme Sayısı ( Zaman Dağılımı )
Görüntülenme
366
09.12.2022 tarihinden bu yana
İndirme
1
09.12.2022 tarihinden bu yana
Son Erişim Tarihi
17 Temmuz 2024 18:57
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copolymer method standard deviation relative factor preconcentration 45 µg L-1 Detection optimized respectively samples Hungary Budapest Kiadó Akadémiai materials reference Adsorption different applied 52 mg g-1 uranium(VI) polymer volume capacity sample proposed chloride-g-dimethyl benzyl poly(caprolactone-b-vinyl methacrylate) uranium determination spectrophotometric
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