Determination of biogenic amines in licorice (Glycyrrhiza glabra) by ion-pair extraction and liquid chromatography–tandem mass spectrometry

BACKGROUND: Ion-pair extraction combined with liquid chromatography–tandem mass spectrometry method has been proposed for the determination of biogenic amines in licorice samples. RESULTS: Limit of detection and limit of quantitation for the biogenic amines were 1.4–2.7 and 4.7–9.1 ng mL-1, respectively. Relative standard deviations based on five replicate extraction of 100 ng mL-1 of each biogenic amine were <4.7% for intra-day and 7.4% for inter-day precision. The method described in this study has been shown to be in accordance with satisfactory accuracy and good reproducibility for the quantitative determination of biogenic amines in licorice samples. Nine biogenic amines (putrescine, cadaverine, histamine, spermine, spermidine, tyramine, tryptamine, agmatine and phenylethylamine) were detected in licorice samples and total biogenic amine concentrations were determined at 369 ng mL-1 in fresh and 3532 ng mL-1 in non-fresh licorice samples. Putrescine was found at the highest concentrations to be up to 704 ng mL-1 in all the analyzed samples, followed by tyramine (675 ng mL-1) and tryptamine (282 ng mL-1). Putrescine, tyramine and spermine concentrations were dramatically increased, whereas agmatine concentration was significantly decreased, in non-fresh licorice samples compared to fresh ones. CONCLUSION: The consumption of freshly prepared licorice is recommended because of the relatively low concentration of total biogenic amines. © 2016 Society of Chemical Industry. © 2016 Society of Chemical Industry

Yazar Ata Ş.
Akyüz M.
Çabuk H.
Yayın Türü Article
Tek Biçim Adres https://hdl.handle.net/20.500.12628/5045
Tek Biçim Adres 10.1002/jsfa.7881
Konu Başlıkları biogenic amines
ion-pair extraction
LC-MS/MS
licorice
Koleksiyonlar Araştırma Çıktıları | WoS | Scopus | TR-Dizin | PubMed | SOBİAD
Scopus İndeksli Yayınlar Koleksiyonu
Dergi Adı Journal of the Science of Food and Agriculture
Dergi Cilt Bilgisi 97
Dergi Sayısı 5
Sayfalar 1427 - 1432
Yayın Yılı 2017
Eser Adı
[dc.title]
Determination of biogenic amines in licorice (Glycyrrhiza glabra) by ion-pair extraction and liquid chromatography–tandem mass spectrometry
Yazar
[dc.contributor.author]
Ata Ş.
Yazar
[dc.contributor.author]
Akyüz M.
Yazar
[dc.contributor.author]
Çabuk H.
Yayın Yılı
[dc.date.issued]
2017
Yayıncı
[dc.publisher]
John Wiley and Sons Ltd
Yayın Türü
[dc.type]
article
Özet
[dc.description.abstract]
BACKGROUND: Ion-pair extraction combined with liquid chromatography–tandem mass spectrometry method has been proposed for the determination of biogenic amines in licorice samples. RESULTS: Limit of detection and limit of quantitation for the biogenic amines were 1.4–2.7 and 4.7–9.1 ng mL-1, respectively. Relative standard deviations based on five replicate extraction of 100 ng mL-1 of each biogenic amine were <4.7% for intra-day and 7.4% for inter-day precision. The method described in this study has been shown to be in accordance with satisfactory accuracy and good reproducibility for the quantitative determination of biogenic amines in licorice samples. Nine biogenic amines (putrescine, cadaverine, histamine, spermine, spermidine, tyramine, tryptamine, agmatine and phenylethylamine) were detected in licorice samples and total biogenic amine concentrations were determined at 369 ng mL-1 in fresh and 3532 ng mL-1 in non-fresh licorice samples. Putrescine was found at the highest concentrations to be up to 704 ng mL-1 in all the analyzed samples, followed by tyramine (675 ng mL-1) and tryptamine (282 ng mL-1). Putrescine, tyramine and spermine concentrations were dramatically increased, whereas agmatine concentration was significantly decreased, in non-fresh licorice samples compared to fresh ones. CONCLUSION: The consumption of freshly prepared licorice is recommended because of the relatively low concentration of total biogenic amines. © 2016 Society of Chemical Industry. © 2016 Society of Chemical Industry
Kayıt Giriş Tarihi
[dc.date.accessioned]
2019-12-23
Açık Erişim Tarihi
[dc.date.available]
2019-12-23
Yayın Dili
[dc.language.iso]
eng
Konu Başlıkları
[dc.subject]
biogenic amines
Konu Başlıkları
[dc.subject]
ion-pair extraction
Konu Başlıkları
[dc.subject]
LC-MS/MS
Konu Başlıkları
[dc.subject]
licorice
Haklar
[dc.rights]
info:eu-repo/semantics/closedAccess
ISSN
[dc.identifier.issn]
0022-5142
İlk Sayfa Sayısı
[dc.identifier.startpage]
1427
Son Sayfa Sayısı
[dc.identifier.endpage]
1432
Dergi Adı
[dc.relation.journal]
Journal of the Science of Food and Agriculture
Dergi Sayısı
[dc.identifier.issue]
5
Dergi Cilt Bilgisi
[dc.identifier.volume]
97
Tek Biçim Adres
[dc.identifier.uri]
https://dx.doi.org/10.1002/jsfa.7881
Tek Biçim Adres
[dc.identifier.uri]
https://hdl.handle.net/20.500.12628/5045
Görüntülenme Sayısı ( Şehir )
Görüntülenme Sayısı ( Ülke )
Görüntülenme Sayısı ( Zaman Dağılımı )
Görüntülenme
27
09.12.2022 tarihinden bu yana
İndirme
1
09.12.2022 tarihinden bu yana
Son Erişim Tarihi
09 Şubat 2024 07:15
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Tıklayınız
biogenic samples licorice amines concentrations tyramine tryptamine agmatine non-fresh Putrescine concentration Chemical determination spermine method Society extraction highest detected determined BACKGROUND CONCLUSION Industry relatively because recommended prepared freshly consumption compared analyzed decreased significantly whereas increased
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