Determination of selected natural hormones and endocrine disrupting compounds in domestic wastewater treatment plants by liquid chromatography electrospray ionization tandem mass spectrometry after solid phase extraction

A new analytical method for the simultaneous determination of two natural hormones (progesterone and estrone) and two selected endocrine disrupter compounds (EDCs) (diltiazem and carbamazepine (Cbz)) was developed by liquid chromatography electrospray ionization tandem mass spectrometry (LC-ESI-MS/MS) after pre-concentration with solid phase extraction (SPE). Influent and effluent samples taken from five different wastewater treatment plants throughout Turkey namely Hurma/Antalya, Lara/Antalya, Kemer-1 and Kemer-2 and METU/Ankara were analyzed for their EDCs contents under the optimum conditions. All of the parameters in the pre-concentration step were optimized and the best recoveries for all compounds of interest were achieved at pH 7 (about 100%). Progesterone was not detected in any of the treatment plants while diltiazem was found in all samples with the exception of Lara effluent. © The Royal Society of Chemistry 2012.

Yazar Muz M.
Selcen Sönmez M.
Komesli O.T.
Bakirdere S.
Gökay C.F.
Yayın Türü Article
Tek Biçim Adres https://hdl.handle.net/20.500.12628/5062
Tek Biçim Adres 10.1039/c2an15644j
Koleksiyonlar Araştırma Çıktıları | WoS | Scopus | TR-Dizin | PubMed | SOBİAD
Scopus İndeksli Yayınlar Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu
Dergi Adı Analyst
Dergi Cilt Bilgisi 137
Dergi Sayısı 4
Sayfalar 884 - 889
Yayın Yılı 2012
Eser Adı
[dc.title]
Determination of selected natural hormones and endocrine disrupting compounds in domestic wastewater treatment plants by liquid chromatography electrospray ionization tandem mass spectrometry after solid phase extraction
Yazar
[dc.contributor.author]
Muz M.
Yazar
[dc.contributor.author]
Selcen Sönmez M.
Yazar
[dc.contributor.author]
Komesli O.T.
Yazar
[dc.contributor.author]
Bakirdere S.
Yazar
[dc.contributor.author]
Gökay C.F.
Yayın Yılı
[dc.date.issued]
2012
Yayın Türü
[dc.type]
article
Özet
[dc.description.abstract]
A new analytical method for the simultaneous determination of two natural hormones (progesterone and estrone) and two selected endocrine disrupter compounds (EDCs) (diltiazem and carbamazepine (Cbz)) was developed by liquid chromatography electrospray ionization tandem mass spectrometry (LC-ESI-MS/MS) after pre-concentration with solid phase extraction (SPE). Influent and effluent samples taken from five different wastewater treatment plants throughout Turkey namely Hurma/Antalya, Lara/Antalya, Kemer-1 and Kemer-2 and METU/Ankara were analyzed for their EDCs contents under the optimum conditions. All of the parameters in the pre-concentration step were optimized and the best recoveries for all compounds of interest were achieved at pH 7 (about 100%). Progesterone was not detected in any of the treatment plants while diltiazem was found in all samples with the exception of Lara effluent. © The Royal Society of Chemistry 2012.
Kayıt Giriş Tarihi
[dc.date.accessioned]
2019-12-23
Açık Erişim Tarihi
[dc.date.available]
2019-12-23
Yayın Dili
[dc.language.iso]
eng
Haklar
[dc.rights]
info:eu-repo/semantics/closedAccess
ISSN
[dc.identifier.issn]
0003-2654
İlk Sayfa Sayısı
[dc.identifier.startpage]
884
Son Sayfa Sayısı
[dc.identifier.endpage]
889
Dergi Adı
[dc.relation.journal]
Analyst
Dergi Sayısı
[dc.identifier.issue]
4
Dergi Cilt Bilgisi
[dc.identifier.volume]
137
Tek Biçim Adres
[dc.identifier.uri]
https://dx.doi.org/10.1039/c2an15644j
Tek Biçim Adres
[dc.identifier.uri]
https://hdl.handle.net/20.500.12628/5062
Görüntülenme Sayısı ( Şehir )
Görüntülenme Sayısı ( Ülke )
Görüntülenme Sayısı ( Zaman Dağılımı )
Görüntülenme
9
09.12.2022 tarihinden bu yana
İndirme
1
09.12.2022 tarihinden bu yana
Son Erişim Tarihi
07 Nisan 2024 21:45
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Tıklayınız
effluent compounds samples treatment plants pre-concentration parameters optimized conditions optimum contents analyzed METU/Ankara recoveries diltiazem Chemistry Society exception interest detected Progesterone (about Kemer-1 achieved Kemer-2 wastewater Lara/Antalya endocrine developed (Cbz)) carbamazepine (diltiazem (EDCs) disrupter selected
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