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(1RS,4RS)-1-Methoxyspiro[bicyclo[2.2.2]oct-5-ene-2,2'-[1', 3']dithiolane]

Gültekin Z. | Adams H. | Hökelek T.

Article | 2003 | Acta Crystallographica Section E: Structure Reports Online59 ( 7 )

The preparation of (1RS,4RS)1-Methoxyspiro[bicyclo[2.2.2]oct-5-ene-2, 2'-[1',3 ']dithiolane] compound by a literature method was shown. The compound consists of a five-membered dithiolane ring with a methoxybicyclooctene spiro-fused at the 2-position. It was observed that the S atom of the dithiolane ring have electron-releasing properties, but the O atom of the methoxy group was electron-withdrawing, thereby influencing the bond lengths and angles of the dithiolane ring. The structure determination of the compound was undertaken to understand the effects of the methoxybicyclo-octene system and to compare the results with those foun . . .d in 1,2,3,4- tetrahydrocarbazole-1-spiro-2'-[1,3]dithiolane Daha fazlası Daha az

(1 RS,3RS)-2-Methoxymethyl-1,3-dithiolane 1,3-dioxide

Özcan Ö. | Gültekin Z. | Frey W. | Hökelek T.

Article | 2003 | Acta Crystallographica Section E: Structure Reports Online59 ( 10 )

The title compound, C5H10O3S2, consists of a five-membered dithiolane ring with one O atom bonded to each S atom and a methoxymethyl group at the 2-position. Some interatomic close contacts appear to influence the geometry of the dithiolane ring. © 2003 International Union of Crystallography Printed in Great Britain - all rights reserved.

2-methoxymethyl-1,3-dithiepane 1,1,3,3-tetraoxide

Gültekin Z. | Frey W. | Hökelek T.

Article | 2003 | Acta Crystallographica Section E: Structure Reports Online59 ( 9 )

The title compound, C7H14O5S2, consists of a seven-membered dithiepane ring with two O atoms bonded to each S atom and a methoxymethyl group at the 2-position. A few close contacts seem to influence the geometry of the dithiepane ring. © 2003 International Union of Crystallography Printed in Great Britain - all rights reserved.

2-Methoxymethyl-1,3-dithiolane 1,1,3,3-tetraoxide

Özcan Ö. | Gültekin Z. | Frey W. | Hökelek T.

Article | 2003 | Acta Crystallographica Section E: Structure Reports Online59 ( 6 )

The title compound, C5H10O5S2, consists of a five-membered dithiolane ring with two O atoms bonded to each S atom and a methoxymethyl group at the 2-position. The asymmetric unit contains two molecules. A few interatomic close contacts seem to influence the geometry of the dithiolane ring. © 2003 International Union of Crystallography Printed In Great Britain - all rights reserved.


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